I-sodium butyl naphthalene sulfonate:
1. Chaza izingxenye ezingu-426 ze-naphthalene ezingxenyeni ezingu-478 ze-n-butanol, engeza izingxenye ezingu-1 060 ze-sulfuric acid egxilile kanye nezingxenye ezingu-320 ze-sulfuric acid evuthayo ngaphansi kokuyaluza. I-Gabi yayishiselwa kancane ibe ngu-50-55 ℃ futhi igcinwe amahora angu-6. Ngemuva kokuma, i-asidi engaphansi iyakhululwa. Isixazululo esingaphezulu sokusabela sincishiswa nge-alkali, bese sixutshwa nge-sodium hypochlorite, i-sedimentation, ukuhlunga, ukufutha nokomisa ukuze uthole umkhiqizo ophelile.
2. Kusuka ku-naphthalene ne-butanol, i-sulfuric acid ngokusabela kwe-sulfonation elungiselelwe:
25638-17-9 ukulungiswa
I-butanol engu-320kg kanye ne-60kg sec-octanol yengezwe ebhodweni lokusabela, yanyakaziswa futhi yapholiswa, kwaphinde kwengezwa i-naphthalene engu-276kg. 1232kg sulfuric acid (98% sulfuric acid 470kg kanye 20% fuming sulfuric acid 762kg) yengezwe phakathi 3h at 40 ~ 45 ℃. Ngemva kokungeza, izofudumeza ngokuzenzakalelayo kufika ku-50 ~ 55℃ phakathi kuka-1.5h futhi ibambe ku-55 ~ 58℃ amahora angu-5. Vumela ume amahora angu-3 bese uhlukanisa i-asidi edoti engxenyeni engezansi. Faka u-500kg wamanzi ukuze uhlanjululwe, upholile ku-40 ~ 50 ℃, faka into ebhakedeni le-neutralization, engeza u-30% we-alkali ewuketshezi ukuze ungathathi hlangothi ngasikhathi sinye, izinga lokushisa lokungathathi hlangothi alidluli ku-60 ℃, lawula inani le-pH liyi-7 ~ 8. I-liquid yezinto ezibonakalayo yomile, iphansi, yengeza i-sodium sulfate yokugaya, futhi i-penetrant standardized BX1100kg iyatholakala.
I-sodium butyl naphthalene sulfonateIkhemikhali yekhompyutha
1. Inani eliyisethenjwa lesibalo sepharamitha ye-hydrophobic (XlogP) : Akukho
2. Inani labanikeli bebhondi ye-hydrogen :0
3. Inombolo yama-hydrogen bond receptors :3
4. Inombolo yamabhondi aphendukayo :5
5. Inombolo yama-tautomer: Akukho
6. Indawo ye-Polar yama-molecule e-topological ingama-51.8
Inani lama-athomu asindayo :19
8. Ukushaja okungaphezulu :0
9. Inkimbinkimbi :345
10. Inombolo ye-athomu ye-Isotope :0
11. Thola inani lezikhungo eziyinhloko zesakhiwo :0
12. Inani lezikhungo ze-athomu ezingaqinisekile :0
13. Thola inani lezikhungo zebhondi yamakhemikhali :0
14. Inani lezikhungo zebhondi yamakhemikhali ezingaqinisekile :0
15. Amayunithi ebhondi ye-Covalent :2
Isikhathi sokuthumela: Jun-20-2022